Slow strain rate (SSR) testing, also known as constant extension
rate testing (CERT), is a modification of the constant load tension
test as shown schematically in Fig. 1. In this case, the constant
load has been replaced by a slow extension of the specimen until
failure. A more detailed description of this test method is given
in ASTM G129. The benefit of SSR testing is that it produces a
result in a reasonably short time, usually within 1-7 days in
most cases, depending on strain rate. It also reduces incubation
time to the onset of cracking in susceptible materials through
the application of the dynamic plastic straining.
The plastic strain causes an accelerated disruption of surface
films thereby overcoming the initial period of incubation that
can result in unacceptably long test durations. However, in some
cases, the plastic strain can add complications to the interpretation
of the test results because most materials are not prone to this
degree of straining in actual service.
The main benefit of the SSR test is that it allows the evaluation
of the effect of metallurgical variables such as alloy composition,
heat treatment and processing and/or environmental parameters
(e.g.. aeration, concentration, inhibition, etc.) in a relatively
short period of testing. Strain rates utilized for SSR testing
are typically in the range of 1- 4 x10-6 s-1.
At a strain rate of 4 x10-6 s-1, the testing
speed is about 1% strain per hour and failure of most engineenng
materials will occur within a day or two. In some cases, slower
strain rates are required.
Additionally. in some cases, longer exposure periods prior to
testing may be necessary if long-term formation of corrosion films
is a critical step in the cracking process. One example of this
effect is the formation of water scales on austenitic stainless
steels, which can exacerbate SCC in chloride-containing waters.
However, in most cases, short-term testing can provide meaningful
data on the roles of many variables on Environmentally Assisted
Cracking (EAC).
Evaluation for susceptibility to EAC is normally obtained through
the comparison of the results of tests conducted in a corrosive
environment vs. corresponding data obtained in an inert environment
(i.e., an environment that has been shown not to promote EAC or
significant corrosion in the material being tested). In most cases
these tests are conducted in air. Direct examination of the specimen
gage section for EAC and documentation of fracture mode are also
important to a full interpretation of the SSR test results. The
SSR test results that are used include time to failure, plastic
elongation to failure, reduction in area, ultimate tensile strength,
and load at fracture. These data are usually presented in terms
of their ratios vs the corresponding value from a test conducted
in an inert environment. Ratios in the range 0.8-1.0 normally
denote high resistance to EAC whereas low values (i.e.< 0.5)
show high susceptibility. In some cases, hydrogen can cause loss
in ductility without indication of brittle cracking in the specimen.
This is usually a less important situation than when direct evidence
of embrirtlement has been observed, particularly if the material
still exhibits a high tensile strength ratio.